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High resolution mass spectra (HRMS) were acquired on a JEOL AccuTOF 4G LC-plus equipped with an ionSense DART (Direct Analysis in Real Time) source for phosphines 1 – 5. HRMS for complexes 1-Cu – 5-Cu were obtained on an Agilent 6545 mass spectrometer coupled to an Agilent Infinity 1260 LC system running a Jet Stream electrospray ionization (ESI) source. DART(+) data may be processed using JEOL software (msAxel data processing). Performing drift compensation is required by referencing PEG(+) a 415.25377. A pdf guide is available at https://chemistry.mit.edu/facilities-and-centers/department-of-chemistry-instrumentation-facility-dcif/ and a local copy dated to 25 May 22 is available. ESI(+) data may be processed using Agilent software (MassHunter Quanlitative Analysis).
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Created: 16th Mar 2023 at 17:15
Last updated: 16th Mar 2023 at 17:23
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Version 1 (earliest) Created 16th Mar 2023 at 17:15 by Charles Demurjian
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