#Item name liquid-liquid extraction and GC/MS-MS in SRM mode Creation date 28-Oct-21 #Extraction Extract ID liquid_extr Extract Name liquid Extraction Method liquid-liquid extraction with 30mL ethyl acetate three times Date Extraction #Post Extraction Derivatization or Labelling none Date Derivatization or Labelling none Derivatized or labeled Extract ID none Derivatized or labeled Extract Name none Other Post Extraction Procedures concentration by rotatory evaporator at room temperature to 1mL and syringe filtration Storage direct analysis #Chromatography Date GC-MS Run %today% GC Instrument Trace 1300 Thermo Scientific GC Autosampler Model AI 1310 Thermo Scientific GC Column model Zebron ZB5-MS GC Column type fused silica capillary column 30mx0.25x0.25 Guard Column none #Mass spectrometry MS Scan polarity positive MS Scan mz range transitions for pheromone compounds 82-67 5eV, 95-67 10eV, 96-54 10 eV and 96-81 5eV MS Instrument TSQ 8000 Evo Thermo Scientific MS Ion source electron ionization (EI) Mass analyzer triple quadrupole mass filter Raw Spectral Data Files Blank #Other Operator Sandra Vacas Notes